Proton NMR spectra were recorded on a JEOL FT-90 MHz spectrometer. ... (1H, s, C-2 aromatic proton), 6.05 (1H, bs, C-7 olefinic proton), 2.7 to. 2.1 (...

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olefinic protons at d 5.25 (1H, d, J 17.0Hz), 5.26 (1H, d,. J 10.8 Hz), 5.59 (1H, d, J 15.8 Hz), 5.70 (1H, dt, J 15.8,. 7.3 Hz) and 5.88 (1H, dd, J 17.0, 10.8 Hz), and ...

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